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Case Studies/Tech Papers
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Whenever the door to a vacuum furnace chamber is open, humidity from the air will enter the chamber and condense in a very thin film on the chamber walls or be absorbed into the hot zone materials.
When the chamber is subsequently evacuated (before heating) and the furnace internals are exposed to this lower pressure, “outgassing” of the entrapped moisture will occur. If sufficient moisture has been entrapped (such as in very humid environments), the outgassing effect will slow the pumpdown process and may even give the appearance of a malfunction in the pumping system. Eventually, the outgassed moisture will be pulled out of the chamber by the pumping system and evacuation rates will improve. This same effect will be apparent when oily or contaminated workloads are placed in the furnace. It may be more pronounced in furnaces with graphite-based hot zone insulation materials. READ MORE
This is the third in a series of four articles on Vacuum Furnace Maintenance. (read part 1) / (read part 2)
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Case Studies/Tech Papers
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During construction, all welded joints in a vacuum furnace are inspected for hermetic integrity and should remain intact for the life of the furnace.
However, there are also a number of demountable connections that can be separated and reconnected for component changing or repair access reasons. These connections are generally sealed with a gasket sandwiched between two flanges. Though different gasket materials are used depending on the vacuum level required, most seals in a standard vacuum furnace incorporate an o-ring made of natural or synthetic rubber. Buna-N, silicone and Viton o-rings are readily available in many sizes. READ MORE
This is the second in a series of four articles on Vacuum Furnace Maintenance. (read part 1)
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Case Studies/Tech Papers
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As with any piece of equipment, proper maintenance at regular intervals is essential for long service life and trouble free operation.
The mechanical components in a vacuum furnace require standard maintenance practices (ie. cleaning, lubrication, etc.). However, successful use of a vacuum furnace depends on the purity and reliability of its vacuum. Additional maintenance activities are required to ensure good vacuum levels in the system. Leaks in joints and contamination of furnace internals will greatly affect operating vacuum levels and the quality of the processing. Leaks are the most time-consuming and troublesome of the maintenance items. READ MORE
This is the first in a series of four articles on Vacuum Furnace Maintenance due to appear over the next three months.
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Case Studies/Tech Papers
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Clean, oxide-free surfaces are essential to achieve sound brazed joints.
Uniform capillary action will occur only when all grease, oil, dirt and oxides have been removed from both the braze alloy and base metal prior to brazing. The length of time that cleaning remains effective depends on the material involved, atmospheric conditions, storage techniques and the amount of handling that may be involved. It is recommended that brazing be performed as soon as possible after the material has been cleaned. The selection of a cleaning technique depends on the nature of the contaminant, the base metals involved and the joint design. The same cleaning practices used for vacuum heat treating (ie. manual cleaning, vapour degreasing, etc.) are applicable to vacuum brazing. READ MORE
This is the third in a series of four articles on Vacuum Brazing Tecniques. (read part 1) / (read part 2)
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Case Studies/Tech Papers
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Brazing involves the joining of two or more base metal components by melting a thin layer of filler metal into the space between them.
Bonding results from the intimate contact produced by the dissolution of a small amount of base metal into the filler metal, without melting of the base metal. Brazing differs from welding, in which the joint is formed through melting of the base metal. Brazing is similar to soldering but, by definition, is performed at higher temperatures. In brazing, the filler metal can be placed within the joint as a foil, or placed over the joint in the form of paste or wire. Joint clearances must be very carefully controlled and usually do not exceed .12mm (.005"). Capillary action draws the molten filler metal into the joint and holds it there. The base metal components must be designed to enhance the capillary action. Brazing is a process that has been well adapted to vacuum heating methods. READ MORE
This is the second in a series of four articles on Vacuum Brazing Tecniques. (read part 1)
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Case Studies/Tech Papers
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Most base metals typically brazed in vacuum furnaces have a natural oxide “coating” that can inhibit the flow of brazing filler metals.
The oxides of the less reactive metals like iron, nickel and cobalt tend to dissociate (break down) under low pressure and high temperature. Therefore, alloys such as the 300 and 400 series stainless steels, carbon steels and many tool steels can be successfully brazed in vacuum at relatively high pressures (1 to 50 microns). READ MORE
This is the first in a series of four articles on Vacuum Brazing Tecniques due to appear over the next three months.
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Case Studies/Tech Papers
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All furnace equipment used for heat treating should be properly instrumented and periodically tested for uniformity.
The temperature uniformity within the furnace must be regularly surveyed. The frequency of surveying is largely dependent on the type of equipment in use and its previous history in accuracy and reliability. Exact survey frequencies should be determined from applicable processing specifications. However, quarterly temperature uniformity surveys are fairly standard. The purpose of the uniformity survey is to determine the range of temperatures present at different locations in the furnace under normal operating conditions. A furnace is normally qualified through an initial comprehensive survey. READ MORE
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