Once a good fixture design has been developed, careful consideration should next be given to the loading of the workpieces.

Heating in a vacuum depends mostly on the transfer of energy through radiation from the elements to the load.  For uniform heating and cooling, it is important that the workpieces are not shielded by one another.  Pieces within the load should be evenly spaced to ensure even exposure to radiation.  The size, shape and high temperature strength of the workpiece should also be considered during loading.  Alloys with complex shapes and relatively low strength at heat treating temperatures may distort during processing.  In some cases, it may be necessary to support these components with specially designed fixtures.

For heat treating purposes, "quenching" can be defined as the rapid cooling of a metal to impart some desired property such as hardness.

Different metals and alloys require different quenching rates to achieve their optimum properties. Regardless of equipment design, gas quenching in vacuum furnaces involve the same basic principles. The gas quenching process normally consists of the following sequence of events. First, the power to the heating elements is shut off. Next, the furnace chamber and quench loop are backfilled with a non-reactive gas, commonly nitrogen or argon.

There are several factors to be considered in preparing workpieces for vacuum heat treating or brazing. Cleanliness of the workpieces and baskets or fixtures is very important.

They must be free of oil, dirt, machining lubricants or other contaminants prior to being loaded into the furnace. Some lubricants contain sulphur compounds which can adversely affect the alloys being heat treated. Inadequate cleaning can also cause staining and discoloring of the end product or result in poor braze alloy flow. Contaminants with high vapour pressures will evaporate during heating causing loss of vacuum. The vapours may eventually condense on colder surfaces in the furnace only to re-vaporize to cause contamination problems in subsequent runs.

When heat treating or brazing in vacuum, the vapour pressure of the constituents in the materials being processed can be a very important consideration. 

The vapour pressure of a material is that pressure exerted at a given temperature when a material is in equilibrium with its own vapour.  Vapour pressure is a function of both the material and the temperature.  Figure 1 shows approximate vapour pressure curves for a variety of metals and compounds.  The area to the left of each curve represents the conditions of temperature and pressure under which the material exists as a solid.  The area to the right of each curve represents those conditions under which the material exists as a gas (or vapour).

In vacuum processing, metal surfaces remain very clean and free of oxides. When these near-perfect surfaces are in contact with other surfaces, certain elements have a tendency to interact between the surfaces through solid state diffusion. Therefore, a major consideration when selecting both hearth and load fixturing materials for vacuum heat treating is the possibility of solid state diffusion between different materials in contact at high temperatures. Solid state diffusion of certain elements can cause the formation of a lower melting point alloy called a eutectic. For example, solid state diffusion between carbon and nickel can begin to occur at temperatures as low as 1165ºC (2130ºF) and cause local melting, also known as eutectic melting.

The air we breathe contains a number of elements that can react with metals under the proper conditions. Moisture, oxygen, carbon dioxide and hydrogen are present in significant amounts in our atmosphere. Each can react to varying degrees with many different metals. While many of these reactions occur to only a small extent at room temperature, they are often greatly accelerated in the presence of heat. Consider the example of a piece of polished metal held over a heat source. It will eventually turn blue or black as the elements in the atmosphere react with the hot metal.

The purchase of a vacuum furnace involves a considerable capital investment. As a result, the question of buying a used furnace at a lower cost than a new furnace is a fairly common one. However, there are a number of potential issues with used equipment that should underscore the warning “buyer beware”. To begin with, good used vacuum furnaces are a rare commodity. When they do appear on the market, they don’t last long. Many of the best are purchased through industry networking and never reach the general market. Still, there are numerous dealers of used furnace equipment with inventories posted on their websites.