In vacuum processing, metal surfaces remain very clean and free of oxides. When these near-perfect surfaces are in contact with other surfaces, certain elements have a tendency to interact between the surfaces through solid state diffusion. Therefore, a major consideration when selecting both hearth and load fixturing materials for vacuum heat treating is the possibility of solid state diffusion between different materials in contact at high temperatures. Solid state diffusion of certain elements can cause the formation of a lower melting point alloy called a eutectic. For example, solid state diffusion between carbon and nickel can begin to occur at temperatures as low as 1165ºC (2130ºF) and cause local melting, also known as eutectic melting.

The air we breathe contains a number of elements that can react with metals under the proper conditions. Moisture, oxygen, carbon dioxide and hydrogen are present in significant amounts in our atmosphere. Each can react to varying degrees with many different metals. While many of these reactions occur to only a small extent at room temperature, they are often greatly accelerated in the presence of heat. Consider the example of a piece of polished metal held over a heat source. It will eventually turn blue or black as the elements in the atmosphere react with the hot metal.

The purchase of a vacuum furnace involves a considerable capital investment. As a result, the question of buying a used furnace at a lower cost than a new furnace is a fairly common one. However, there are a number of potential issues with used equipment that should underscore the warning “buyer beware”. To begin with, good used vacuum furnaces are a rare commodity. When they do appear on the market, they don’t last long. Many of the best are purchased through industry networking and never reach the general market. Still, there are numerous dealers of used furnace equipment with inventories posted on their websites.

Establishing a new heat treating capability requires a significant capital investment in furnace equipment. However, there are other important issues that should be considered. VAC AERO has prepared a few brief guidelines to assist you in establishing this capability